Course Profile   Chemistry (SCH4U), Grade 12, University Preparation, Public

 

Unit 1:  Chemical Systems and Equilibrium

Time:  30 hours

 

Activity 1.1 | Activity 1.2 | Activity 1.3 | Activity 1.4 | Activity 1.5 | Activity 1.6

 

Unit Description

In this unit, students increase their understanding of solutions to incorporate equilibrium systems. Students investigate the behaviour of different equilibrium systems, e.g., liquid-vapour, insoluble salts, weak acids and bases, and solve problems involving the law of chemical equilibrium. Le Chatelier’s principle is used to predict how various factors affect a chemical system at equilibrium. Students explore the importance of equilibrium systems in their daily lives, e.g., how they optimize the production of industrial chemicals and the role they play in biological systems. Throughout the unit, the increased encouragement and emphasis is placed on independent learning strategies, e.g., students generate their own notes and compare them with teacher expectations. In the End-of-Unit Task, students use their titration skills and their understanding of molar solubility and the common ion effect to determine an unknown concentration. Students also complete a written test.

Unit Synopsis Chart

Activity/ Time

Learning Expectations

Assessment Categories

Task/Focus

1.1
An Introduction to Equilibrium Systems

10 h

CSV.01, CSV.02, CSV.03, CS1.01, CS1.02, CS1.03, CS1.07, CS2.01, CS2.02, CS2.03, CS2.06, CS3.01
SIS.01, SIS.02, SIS.03, SIS.07, SIS.08, SIS.09

Knowledge/ Understanding
Inquiry
Communication
Making Connections

Diagnostic carousel activity; teacher-led discussions; student-designed investigations and reporting; graphical analysis; seminar on practical applications of Le Chatelier’s principle; applications of problem-solving equilibrium systems.

1.2
Entropy

2 h

CSV.01, CS1.04, CS1.05

Knowledge/ Understanding
Communication

Teacher demonstration; teacher-led discussion; independent note taking; environmental application.

1.3
Solubility of Salts

6 h

CSV.01, CSV.02, CS1.06, CS1.07, CS2.01, CS2.03, CS2.04, CS2.05, CS2.06, CS3.02
SIS.01, SIS.02, SIS.03, SIS.08, SIS.09, SIS.10

Knowledge/ Understanding
Inquiry
Making Connections
Communication

Teacher-directed lesson; student laboratory exercise; problem solving applications; practical applications of solubility.

1.4
Acid Base Equilibrium

6 h

CSV.01, CSV.02, CS1.07, CS1.08, CS2.01, CS2.03, CS2.06, CS2.07, CS2.08
SIS.01, SIS.02, SIS.03, SIS.09

Knowledge/ Understanding
Inquiry
Communication
Making Connections

Teacher-directed lesson; student-designed titration experiment; independent note taking; problem solving.

1.5
Buffer Solutions

2.5 h

CSV.01, CSV.03, CS1.09, CS3.03
SIS.06

Knowledge/ Understanding
Inquiry
Making Connections
Communication

Teacher demonstration; research and seminar on how buffering action impacts daily life.

1.6
End-of-Unit Task and Written Test

3.5 h

CSV.01, CSV.02, CSV.03
SIS.01, SIS.02, SIS.03

Knowledge/ Understanding
Inquiry
Making Connections
Communication

Students design, conduct and report on an equilibrium experiment; written test.

Unit Planning Notes

Some of the planning notes below relate to the content of the unit while others are suggested to help establish routines in this first unit of the course.

·     Follow all board policies/procedures for the safe handling and disposal of chemicals and ensure proper laboratory safety (goggles, gloves, ventilation) for all lab activities.

·     Provide reminder, hints, and personal reflection time on a continual basis for students to generate possible research questions/ideas for the Final Assessment Task.

·     Promote independent learning skills by encouraging students to accept increasing responsibility for their work, e.g., check posted solutions, generate and compare lesson/text notes, formulate scientific questions and participate in peer assessment.

·     It may be appropriate to use a lecture for content delivery occasionally to help better prepare students for university teaching strategies.

·     If possible, book class time in the library/resource centre and/or the computer lab.

·     This unit is rich in problem-solving opportunities. Careful planning will be essential. Consult with math teachers regarding problem-solving background and possible additional/supporting activities; if needed, arrange for possible sharing of the graphing calculators.

·     Collect exemplars of student work, e.g., notes, lab reports, Final Assessment Report, etc. for future reference.

·     Prepare solutions required for the End-of-Unit Task, e.g., Ca(OH)2 and Ca(OH)2 with a dissolved calcium salt such as Ca(NO3)2 at least one week prior to the activity.

·     This unit has a larger proportion of laboratory explorations to better prepare students for the Final Assessment Task.

·     Self- and peer assessment can be used as a valuable component of the assessment for many of the activities, especially when accompanied by clear criteria; evaluation and assignment of marks remain the responsibility of the teacher.

Unit Resources

Jaeger, Dave and Suzanne Weisker. Holt Chemistry: Visualizing Matter Laboratory Experiments. United States: Holt, Rinehart and Winston, Inc., 1996. ISBN 0-03-095284-0

Jenkins, Frank, et al. Nelson Chemistry. Nelson Canada, 1993. ISBN 0-017-603863-9

Slater, Alan and Geoff Rayner-Canham. Microscale Chemistry Laboratory Manual. Don Mills, ON. Addison-Wesley Publishers Ltd., 1994. Teacher’s Edition ISBN 0-201-60216-4 and Student’s Edition ISBN 0-201-60215-6

Tocci, Salvatore and Claudia Viehland. Holt Chemistry: Visualizing Matter. United States: Holt, Rinehart and Winston, Inc., 1996. ISBN 0-03-000193-5

Tocci, Salvatore and Claudia Viehland. Holt Chemistry: Visualizing Matter Study Guide. United States: Holt, Rinehart and Winston, Inc., 1996. ISBN 0-03-095283-2

Toon, Ernest R., et al. Foundations of Chemistry. Canada: Holt, Rinehart and Winston of Canada, Limited, 1990. ISBN 0-03-922287-X

BioChemLinks – http://biochemlinks.com.

Lab safety, teaching science, science-related careers Curriculum Services Canada
Ontario Curriculum Centre –
http://www.curriculum.org
Grade 10 Academic Science Profile Note-Taking Styles

Science Teachers’ Resource Center (Lapeer County Information Depot)
– http://chem.lapeer.org/Chem1Docs/Index.html

The Squier Group – http://www-wilson.ucsd.edu/education/gchem/equilibrium/

Clearinghouse For Science, Mathematics, and Environmental Education – http://www.ericse.org/

Mansfield University – http://www.mnsfld.edu/~bganong/102.html

Wilton Highschool Chemistry – http://www.chemistrycoach.com/

Chemistry Learning Center – http://learn.chem.vt.edu/tutorials/organic/index.html

American Chemical Society
http://chemistry.org/portal/Chemistry?PID=acsdisplay.html&DOC=vc2\1rp\rp1_markers.html
– http://www.sasked.gov.sk.ca/docs/chemistry/mission2mars/ – equilibrium activities

 

Activity 1.1:  An Introduction to Equilibrium Systems

Time:  10.0 hours

Description

This activity introduces students to the concept of dynamic equilibrium. They carry out an experiment to determine the equilibrium constant for a system, followed by solving equilibrium problems involving concentrations of reactants and products and Keq. There is an opportunity to incorporate the use of available technology, e.g., graphing calculators and spectrophotometers. Students develop an understanding of Le Chatelier’s principle and use it to predict the direction in which a system at equilibrium will shift when volume, pressure, concentration, or temperature is changed, and to investigate how it may be applied to optimize the production of industrial chemicals. Students review the expectations for senior formal laboratory writing, in preparation for the End-of-Unit and Final Performance Task.

Strand(s) & Learning Expectations

Strand(s):  Chemical Systems and Equilibrium

Learning Expectations

CSV.01 - demonstrate an understanding of the concept of chemical equilibrium, Le Chatelier’s principle, and solution equilibria;

CSV.02 - investigate the behaviour of different equilibrium systems, and solve problems involving the law of chemical equilibrium;

CSV.03 - explain the importance of chemical equilibrium in various systems, including ecological, biological, and technological systems;

CS1.01 - illustrate the concept of dynamic equilibrium with reference to systems such as liquid-vapour equilibrium, weak electrolytes in solution, and chemical reactions;

CS1.02 - demonstrate an understanding of the law of chemical equilibrium as it applies to the concentrations of the reactants and products at equilibrium;

CS1.03 - demonstrate an understanding of how Le Châtelier’s principle can predict the direction in which a system at equilibrium will shift when volume, pressure, concentration, or temperature is changed;

CS1.07 - define constant expressions; such as Ksp, Kw, Ka, and Kb;

CS2.01 - use appropriate vocabulary to communicate ideas, procedures, and results related to chemical systems and equilibrium;

CS2.02 - apply Le Chatelier’s principle to predict how various factors affect a chemical system at equilibrium, and confirm their predictions through experimentation;

CS2.03 - carry out experiments to determine equilibrium constants;

CS2.06 - solve equilibrium problems involving concentrations of reactants and products and Keq;

CS3.01 - explain how equilibrium principles may be applied to optimize the production of industrial chemicals;

SIS.01 - demonstrate an understanding of safe laboratory practices by selecting and applying appropriate techniques for handling, storing, and disposing of laboratory materials, and using appropriate personal protection;

SIS.02 - select appropriate instruments and use them effectively and accurately in collecting observations and data;

SIS.03 - demonstrate the skills required to plan and carry out investigations using laboratory equipment safely, effectively, and accurately;

SIS.04 - demonstrate a knowledge of emergency laboratory procedures;

SIS.05 - select and use appropriate numeric, symbolic, graphical, and linguistic modes of representation to communicate scientific ideas, plans, and experimental results;

SIS.07 - communicate the procedures and results of investigations for specific purposes by displaying evidence and information, either in writing or using a computer, in various forms, including flow charts, tables, graphs, and laboratory reports;

SIS.08 - express the result of any calculation involving experimental data to the appropriate number of decimal places or significant figures;

SIS.09 - select and use appropriate SI units.

Prior Knowledge & Skills

·     Understanding of the Solutions and Solubility unit from SCH3U

·     Ability to solve quadratic equations

Planning Notes

·     Review and follow all board regulations for the safe handling and disposal of chemicals, e.g., nitric acid. Teachers should consult (WHMIS) Material Safety Data Sheets for appropriate treatment of sensitivities to substances being used in the laboratory.

·     Gather samples of relevant versus irrelevant or testable versus not testable research questions.

·     Prepare a diagnostic quiz based on information from SCH3U if desired for this unit.

·     Based on the outcome of the diagnostic assessment the teacher may wish to develop independent study packages to help strengthen student background knowledge.

·     Gather and prepare materials required for the following Activities: 1.1.3 - straws of different diameter, 50 mL graduated cylinders; 1.1.4 - iodine and bromine tubes, sodium chloride, acetic acid, calcium carbonate; 1.1.6 - hydrated cobalt chloride, chromate/dichromate solutions etc.; 1.1.8 - pipettes, volumetric flasks, spectrophotometers if available, Fe(NO3)3, KSCN, nitric acid.

·     Suggested Note-Taking Styles are provided in the Grade 10 Academic Profile Teacher Support Material - page 3.

·     Prepare questions (and solutions) that incorporate practical applications and career components for the following Activities: 1.1.7 and 1.1.9.

·     Prepare lesson notes for Activity 1.1.5.

·     Plan such that the entire first period may be used to stimulate student interest, e.g., Act 1.1.1 Carousel Activity.

Teaching/Learning Strategies

1.1.1 Student Activity: Students rotate through a carousel of activities to help the teacher assess prior knowledge and prepare a review of concepts and skills required for this unit.

Teacher Facilitation: The teacher prepares a carousel of activities including hands-on and pen-and-paper activities, based on material covered in SCH3U, e.g., binary nomenclature; mole calculations; concentration calculations; solubility rules; processes involved in dissolving compounds; identifying ionic and covalent compounds; titration skills and net ionic equations; formulae of various acids and bases; Bronsted-Lowry and Arrhenius definitions of acids and bases; writing equations for dissociation of acids and bases; operational definition of pH; saturated/unsaturated/super-saturated solution. Depending on the outcomes of the diagnostic activity, the teacher may wish to offer support material to be completed independently.

1.1.2 Student Activity: Students are introduced to the assessment and evaluation strategies for the course, including the midterm examination (if planned) to take place after the second unit and the nature of the End-of-Unit Task. The End-of-Unit Task (Act 1.6) requires students to use their knowledge of Ksp and the common ion effect to design and conduct an experiment. The Final Assessment Task provides senior students with the opportunity to demonstrate their Knowledge and Inquiry, Communication and Making Connections skills at a pre-university level. Students formulate their own research question, keep a log of their time, design and conduct the experiment, and communicate their research in a formal lab report. Students review a rubric and format for a senior level formal laboratory report. In preparation for the Final Assessment Task, students complete a T-chart comparing relevant versus irrelevant, or testable versus not testable research questions. Time is allowed for students to ask clarification questions.

Teacher Facilitation: The teacher reviews the four categories in the Achievement Chart, and emphasizes the importance of independent inquiry skills for the End-of-Unit Task. Assist students with the comparison chart by providing some criteria for an appropriate research question. It is important to guide students to generate a research question for the Final Assessment Task, preferably by the end of the second unit. Their question should relate to or extend upon the topics of study in the course. Be prepared to provide hints to generate appropriate research questions throughout the course. The teacher prepares a handout outlining the format for a formal laboratory report and a corresponding rubric. Suggestions for creating the rubric are found in the Appendix. The teacher recommends that students keep the rubric and format outline accessible in their notes.

1.1.3 Student Activity: Students work with a partner to construct a physical analogue for an equilibrium system. Each student gathers a 50 mL graduated cylinder and a straw (both straws should be identical). One student labels the graduated cylinder ‘Reactant’ and adds 50 mL of water. The other student labels the cylinder ‘Product’ and leaves it empty. Both students place the straw in the graduated cylinder until the bottom of the straw touches the bottom of the cylinder. They then transfer water from their graduated cylinders simultaneously, using one index finger to retain water in the straw. There will be no water transferred from the Product to Reactant containers during the first trial. Students record the volumes of the Reactant and Product after each trial and plot the data as a line graph (plot the Reactant and Product volumes on the same graph). Students formulate questions, design a procedure, and conduct a lab investigating how changing various factors may impact the physical analogue of the equilibrium system that they created. They then analyse and compare the graphical data.

Teacher Facilitation: The teacher provides instructions for the first part of the activity and encourages students to formulate questions investigating how changing various factors may impact the equilibrium system, e.g., starting with equal volumes of Reactant and Product, using straws with different diameters, using two straws in one direction only, etc. Graphing calculators could be used if available. The teacher uses the class results to introduce and explain the concept of equilibrium and to discuss factors that may prevent a reaction from reaching completion.

1.1.4 Student Activity: Students review the criteria for the Observation section of a formal lab report. They then design their own observation chart and collect data while investigating dynamic equilibrium at various lab stations. Students assess one another’s observation charts.

Teacher Facilitation: As part of the progression towards producing independent learners, the teacher discusses expectations for an efficient observation chart with the students, by referring to a rubric or other recording tool. The teacher then sets up a variety of lab stations investigating chemical and physical equilibrium systems, e.g., Cr2O72- and CrO42-, N2O4 and NO2, equilibrium of soluble salt in solvent (NaCl in water), slightly soluble salt in solvent (CaCO3 in water), liquid-vapour equilibrium (bromine tubes), solid-vapour equilibrium (iodine tubes), weak electrolytes in solution.

1.1.5 Student Activity: Students participate in a class discussion about various Note-Taking Styles, e.g., graphic organizers, point form, paragraph form, embedded notes. They generate their own notes based on a teacher-directed lesson about equilibrium and compare them with the teacher’s notes.

Teacher Facilitation: The teacher may wish to direct students to the Grade 10 Academic Profile Teacher Support Material – page 3 on Note Taking Styles and participate in a brief discussion. The teacher directs a lesson on dynamic equilibrium systems including equilibrium constant expressions, and the differences among between Keq, Kp and Kc. The teacher may post lecture notes as a reference and learning tool for students. Collect exemplars from students for future reference material.

1.1.6 Student Activity: Students review the assessment for the Procedure and Result sections of a formal lab report prior to the activity. They investigate Le Chatelier’s principle by designing and conducting a lab to analyse the effect of changing various factors, e.g., temperature, concentration, volume and pressure, on different chemical equilibrium systems. Students participate in a discussion about Le Chatelier’s Principle.

Teacher Facilitation: The teacher reviews requirements for a Formal Laboratory Report and ensures required materials are available for the experiments, e.g., hydrated cobalt chloride to observe the impact of temperature changes; chromate/dichromate to observe the impact of pH changes, etc. The teacher leads a discussion to summarize student results and reviews Le Chatelier’s principle.

1.1.7 Student Activity: Students complete problems based on Le Chatelier’s Principle. They research the application of Le Chatelier’s Principle to optimize production of industrial chemicals, e.g., ammonia, sulphuric acid. Working in small groups, students discuss their findings.

Teacher Facilitation: The teacher assigns problems incorporating practical applications of Le Chatelier’s Principle and possible career connections. Solutions to the problems are posted and students are given an opportunity to ask questions. The teacher may wish to book time in the library and/or computer room to assist students with their research.

1.1.8 Student Activity: Students vary the equilibrium concentrations of a chemical system to qualitatively investigate the effect on chemical equilibrium and to quantitatively determine the equilibrium constant of the system. They compare their results with each other and expected values.

Teacher Facilitation: There is an opportunity for the teacher to incorporate technology into this activity, i.e., Spectrophotometric Determination of the Equilibrium Constant (see Resources).

1.1.9 Student Activity: Students participate in a class discussion about the results of Act. 1.1.8. They discuss possible sources of error. Students solve equilibrium problems involving reactant/product concentrations and equilibrium constants.

Teacher Facilitation: The teacher leads the class in a discussion about Act.1.1.8 and encourages students to formulate ideas about possible sources or error. The teacher provides students with sample solutions to Keq problems. Assign questions involving concentrations of reactants and products and equilibrium constants. The teacher may encourage the use of graphing calculators and the quadratic equation to analyse Keq equations. Solutions should be posted for students to self-assess. The teacher may collect some problems for evaluation or provide a quiz.

Assessment & Evaluation of Student Achievement

A question-answer sheet and a checklist assessing skills could accompany the diagnostic activity to determine the students’ incoming abilities. The teacher could assess one or two categories for each of the four experiments, e.g., Act 1.1.3 - Designing a Procedure and Tables and Figures, Act 1.1.4 - Observations, Act.1.1.6 - Procedure and Results, Act.1.1.8 - Discussion. Peer- and self-assessment could be used for self-generated notes. This activity provides an opportunity to assess and give feedback to students on their note-taking abilities and inquiry skills including laboratory writing skills, which they may apply in the Final Assessment Task. This activity provides many opportunities to assess the students’ Scientific Investigative Skills to help set the tone early in the course. Solutions to selected problems may be evaluated; evaluation of a quiz would serve the same purpose.

Reports (Inquiry, Communication, Making Connections)
Problem Set or Quiz (Knowledge/Understanding, Making Connections, Communication)

Accommodations

·     Allow increased time for the completion of problems or reduce the number of questions as appropriate for some students.

·     Establish a glossary of terms that might be found in notes, texts, and problems.

·     Include diagrams with problems.

·     Alternative note-taking methods such as using a tape recorder can be used.

Resources

– http://129.93.84.115/Chemistry/DoChem/DoChem115.html
Le Chatelier’s Principle

– http://chem.lapeer.org/Chem2Docs/KeqLab.html
Spectrophotometric determination of equilibrium constant

– http://www.cvgs.k12.va.us/research/paper/question.htm
Criteria for a relevant research question

 

Activity 1.2:  Entropy

Time:  2.0 hours

Description

This activity introduces students to changes in entropy associated with chemical and physical processes and the tendency of reactions to achieve minimum energy and maximum entropy. Students investigate the role entropy plays in the spread and elimination of pollutants such as PCBs. They peer assess and check self-generated notes against the teacher’s to help develop confidence in their abilities to work independently.

Strand(s) & Learning Expectations

Strand(s):  Chemical Systems and Equilibrium

Learning Expectations

CS1.04 - identify, in qualitative terms, entropy changes associated with chemical and physical processes;

CS1.05 - describe the tendency of reactions to achieve minimum energy and maximum entropy.

Prior Knowledge & Skills

·     Understanding of physical/chemical changes and endothermic/exothermic reactions.

Planning Notes

·     Prepare lesson notes on entropy.

·     Prepare a rubric for peer assessment of entropy notes.

·     The teacher may wish to gather and prepare materials required for Activity 1.2.1- NaHCO3, bunsen burner, ice, concentrated H2SO4.

·     The teacher should follow all board regulations for the safe handling and disposal of chemicals, e.g., sulphuric acid.

Teaching/Learning Strategies

1.2.1 Student Activity: Students generate their own notes from a teacher demonstration and teacher directed lesson on entropy. Students peer-assess their notes in class and may compare with teacher notes outside of class time. They complete assigned reading and questions.

Teacher Facilitation: Use a demonstration to identify entropy changes associated with physical and chemical processes, e.g., compare the entropies of the solid, liquid, and gaseous states of a substance, concentrated sulphuric acid in water, decomposition of sodium bicarbonate and provide students with an opportunity to formulate and ask questions. Direct a lesson to emphasize that reactions have a tendency to achieve minimum energy and maximum entropy and that entropy is the driving force behind endothermic reactions. Assign problems incorporating environmental issues, e.g., the difficulty associated with eliminating a pollutant such as PCB because of the enormous energy requirement and generation of disorder.

Assessment & Evaluation of Student Achievement

This activity is an opportunity for peer assessment; in addition, provide feedback to students on their note-taking skills.

Notes (Knowledge/Understanding, Communication)

Accommodations

·     Continue to add terms to glossary.

·     Display posters of different note-taking styles, with a description of pluses and minuses for each method.

·     Use a tape recorder for note taking.

Resources

Science Teachers’ Resource Centre Lapeer County Information Depot
– http://learn.chem.vt.edu/tutorials/

 

Activity 1.3:  Solubility of Salts

Time:  6.0 hours

Description

Students perform an experiment to determine the Ksp value of a slightly soluble salt. Students solve a variety of problems involving Ksp including predicting the formation of precipitates and determining the molar solubility of a pure substance in a solution of a common ion. The application and effects of solubility in a variety of contexts are discussed. Students generate their own notes and check posted solutions.

Strand(s) & Learning Expectations

Strand(s):  Chemical Systems and Equilibrium

Learning Expectations

CS2.01 - use appropriate vocabulary to communicate ideas, procedures, and results related to chemical systems and equilibrium (e.g., homogeneous, common ion, Ka value);

CS2.03 - carry out experiments to determine equilibrium constants (e.g., Keq for iron [III] thiocyanate, Ksp for calcium hydroxide, Ka for acetic acid);

CS2.04 - calculate the molar solubility of a pure substance in water or in a solution of a common ion, given the solubility product constant (Ksp), and vice versa;

CS2.05 - predict the formation of precipitates by using the solubility product constant;

CS2.06 - solve equilibrium problems involving concentrations of reactants and products and the following quantities: Keq, Ksp, Ka, Kb, pH, pOH;

CS3.02 - identify effects of solubility on biological systems (e.g., kidney stones, dissolved gases in the circulatory system of divers, the use of barium sulfate in medical diagnosis);

SIS.01 - demonstrate an understanding of safe laboratory practices by selecting and applying appropriate techniques for handling, storing, and disposing of laboratory materials, and using appropriate personal protection;

SIS.02 - select appropriate instruments and use them effectively and accurately in collecting observations and data;

SIS.03 - demonstrate the skills required to plan and carry out investigations using laboratory equipment safely, effectively, and accurately;

SIS.08 - express the result of any calculation involving experimental data to the appropriate number of decimal places or significant figures;

SIS.09 - select and use appropriate SI units;

SIS.10 - identify and describe science-and technology-based careers related to the subject area under study.

Prior Knowledge & Skills

·     Quantities in Chemical Reactions and Solutions and Solubility from SCH3U.

Planning Notes

·     Review and follow all local Board regulations for the safe handling and disposal of chemicals.

·     Gather materials for the following Activities: 1.3.2-silver acetate or lead(II) chloride needs to be prepared several days in advance of the activity; 1.3.4-ammonium hydroxide, ammonium chloride and phenolphthalein and a petri dish.

·     Have students prepare Act 1.3.2 24 hours in advance of making quantitative observations to ensure that all the silver or lead(II) ions have had the opportunity to react.

·     Due to toxic nature of lead(II) chloride, it is suggested that calcium hydroxide be used.

·     Gather and prepare questions (and solutions) that incorporate practical applications and career components for the following Activities: 1.3.3 and 1.3.4.

·     Take proper safety precautions when using concentrated stock solutions.

·     Prepare notes on the applications of solubility product constants.

Teacher/Learning Strategies

Act 1.3.1 Student Activity: Students generate their own notes from a lesson on the equilibrium constant for slightly soluble ionic substances and its applications in the environment, society and industry. They investigate possible related careers. Students set up their lab for Act. 1.3.2 and, based on the lab procedure provided by the teacher, prepare their own observation tables. Students assess each other’s lesson notes outside class time.

Teacher Facilitation: To provide a context for learning the solubility product constant, the teacher refers to applications of equilibrium solubility such as kidney stones, dissolved gases in the circulatory system of divers, the use of barium sulfate in medical diagnosis, the formation of stalactites and stalagmites as found in the Bonnechere Caves in Ontario, hard water and water softeners, refining nickel, developing camera film, and the massive deposits of limestone and gypsum as oceans dry up. A more detailed treatment of these applications can occur in Act 1.3.5 once students have mastered the concept of Ksp and the common ion effect. Based on the results of the diagnostic quiz in Act 1.1.2, the teacher uses the students’ prior knowledge of unsaturated, saturated and supersaturated solutions and links it to chemical equilibrium systems. Students will apply this knowledge in Act 1.3.2 to determine an actual Ksp value. The teacher provides students with the lab procedure for Act 1.3.2.

1.3.2 Student Activity: Students conduct a lab to quantitatively determine the Ksp value for a relatively insoluble salt, e.g., silver acetate by displacement with copper wire, lead(II) chloride with a strip of zinc metal.

Teacher Facilitation: The teacher could set up the analysis section of this lab to lead students step-by-step to arrive at the expression and value for the Ksp of silver acetate or lead(II) chloride. The teacher may quickly check students’ observation tables.

1.3.3 Student Activity: Students solve Ksp questions.

Teacher Facilitation: The teacher should choose Ksp problems involving concentration, including molar solubility of pure substances in water. Problems could be collected for evaluation.

1.3.4 Student Activity: Students take notes on the common ion effect, precipitation reactions, predicting precipitate formation using Ksp data and applications from a teacher-directed lesson. Students solve problems involving common ion effect and compare their answers to posted solutions.

Teacher Facilitation: The teacher could do a quick demonstration of common ion effect such as how an excess of ammonium ions reduces the concentration of hydroxide ions. To do so place a petri dish on an overhead projector, and fill it halfway with 1mol/L ammonium hydroxide. Add two drops of phenolphthalein. The solution should be red. Stir a little solid ammonium chloride into the solution; the red colour will disappear. The ammonium ions suppress the ionization of the ammonium hydroxide. An example of a practical use of equilibrium constants is in the use of barium sulfate as an X-ray contrast medium. Doctors must make certain that almost no poisonous barium ions are present to dissolve in a person’s body fluids. Knowing the solubility product constant for barium sulfate, calculations are made to determine the amount of barium sulfate needed for the procedure. To ensure that the concentration of barium ions will not exceed the safety level, a soluble salt such as sodium sulfate, which contributes sulfate ions, is added to increase the sulfate ion concentration and reduce the barium ion concentration. Because sulfate ion is present in both barium sulfate and sodium sulfate, sulfate is the common ion present in both substances dissolved in the solution. Some students will have trouble grasping the concept of the common ion effect. First, remind them that because the solubility of barium sulfate is very low, it is not involved in the equation for the solubility product constant. It follows that the product of the two ion concentrations is equal to the constant, Ksp. A constant value cannot change, so if one of the concentrations rises, the other must drop. By means of this principle, the common ion effect can be used to increase or decrease the concentration of a chosen ion.

1.3.5 Student Activity: Students can generate their own notes from a more detailed lesson on the practical applications of solubility equilibrium.

Teacher Facilitation: The teacher prepares lesson notes for those applications mentioned in Activity 1.3.1. The teacher administers a quiz based on Solubility Equilibrium.

Assessment & Evaluation of Student Achievement

A lab report (emphasizing the abstract) for the experiment would be appropriate. Short quiz questions on a variety of Ksp problems should be used to determine the students’ abilities and/or a problem set could be collected.

Report (Inquiry, Communication, Making Connections)
Quiz (Knowledge/Understanding, Making Connections, Communication)
Problem Set (Knowledge/Understanding, Making Connections, Communication)

Accommodations

·     Use alternative note-taking methods such as a tape recorder.

·     Reduce the number of repetitive problems.

·     Add terms to glossary.

·     Organize problems according to type and provide model solutions for each type.

Resources

Newton, David. Chemistry Problems. Portland, Maine: J. Weston Walch, Publisher, 1977.

World of Chemistry, TVO Video Series, 1988 – World of Chemistry: Driving Forces

 

Activity 1.4:  Acid Base Equilibrium

Time:  6.0 hours

Description

Students are introduced to the key concept of dissociation constants as a measure of the relative strength of weak acids and bases. They conduct experiments to find the Ka of a weak acid and the pH of salts of weak acids and bases. Students are provided with an opportunity to practise preparing solutions and using titration skills that may be applied in the End-of-Unit and Final Assessment Tasks. They solve a variety of problems involving acid-base equilibrium and titration data.

Strand(s) & Learning Expectations

Strand(s):  Chemical Systems and Equilibrium

Learning Expectations

CS2.01 - use appropriate vocabulary to communicate ideas, procedures, and results related to chemical systems and equilibrium;

CS2.03 - carry out experiments to determine equilibrium constants (e.g., Keq for iron [III] thiocyanate, Ksp for calcium hydroxide, Ka for acetic acid);

CS2.06 - solve equilibrium problems involving concentrations of reactants and products and the following quantities: Keq, Ksp, Ka, Kb, pH, pOH;

CS2.07 - predict, in qualitative terms, whether a solution of a specific salt will be acidic, basic, or neutral;

CS2.08 - solve problems involving acid-base titration data and the pH at the equivalence point;

SIS.01 - demonstrate an understanding of safe laboratory practices by selecting and applying appropriate techniques for handling, storing, and disposing of laboratory materials, and using appropriate personal protection;

SIS.02 - select appropriate instruments and use them effectively and accurately in collecting observations and data;

SIS.03 - demonstrate the skills required to plan and carry out investigations using laboratory equipment safely, effectively, and accurately;

SIS.09 - select and use appropriate SI units.

Prior Knowledge & Skills

·     Properties of acids and bases

·     Bronsted-Lowry and Arrhenius definitions of acids and bases

·     The difference between strong and weak acids and bases in terms of degree of dissociation

·     The operational definition of pH

·     Writing equations for dissociation of acids and bases

·     Basic titration skills

Planning Notes

·     Gather and prepare materials for the following Activities: 1.4.1 – solutions of strong and weak acids and bases, pH meters/probes/paper; 1.4.3 – a number of salts, distilled water and pH meters/probes/paper and a fill-in-the blank worksheet; 1.4.5 – concentrated acid and base solutions, pH meters/probes/paper, indicators and titration apparatus; 1.6 – End-of-Unit Task solutions of Ca(OH)2 and Ca(OH)2 with dissolved calcium salt.

·     Prepare a rubric to assess the Abstract and Discussion sections of a senior-level formal lab report. Some suggested criterion statements are provided in the Appendix.

·     Prepare a peer-assessment checklist for titration skills for use in Act 1.4.5.

·     Gather and prepare questions (and solutions) that incorporate practical applications and career components for the following Activities: 1.4.2, 1.4.3, and 1.4.6.

·     Take proper safety precautions when using concentrated stock solutions.

·     Follow all board regulations for the safe handling and disposal of chemicals.

Teacher/Learning Strategies

1.4.1 Student Activity: Students could generate their own notes to distinguish between strong and weak acids and bases using the concept of equilibrium. Through a teacher-directed lesson, they are introduced to the equilibrium constants Ka, and Kb and Kw.

Teacher Facilitation: Based on the results of the diagnostic quiz in Act 1.1.2, the teacher uses students’ prior knowledge to explain how dissociation constants are a measure of the relative strength of weak acids and bases. The teacher may wish to do a demonstration as a visual aid using pH meters/probes/paper and a variety of solutions of acids and bases to compare strong and weak acids and bases using the concept of equilibrium. This leads to a discussion on equilibrium constants. Remind students that they worked with equilibrium constants in Act 1.1.9 and that the acid/base/water dissociation constants are set up the same way.

1.4.2 Student Activity. Students solve problems calculating pH, [H3O+], pOH, [OH-], Ka, Kb, and Kw.

Teacher Facilitation: Direct a lesson to provide sample questions and solutions for problems calculating pH, [H3O+], pOH, [OH-], Ka, Kb, and Kw. Post answers for the problem set and provide students with an opportunity to ask questions pertaining to the problems. Suggest that experiments to determine equilibrium constants, Kb, Ka for weak acids and bases at various temperatures would be a straightforward Final Assessment Task project.

1.4.3 Student Activity: Students prepare aqueous solutions of several salts and measure the pH of the solutions. Students record their results and then apply their knowledge to homework questions. Students compare their answers to posted solutions.

Teacher Facilitation: In order to encourage students to make connections, the teacher can extend the topic of salt hydrolysis with a discussion of the practical application of antacids to relieve acid indigestion. Excess stomach acid must be treated with a basic solution in order for neutralization to occur. The teacher could bring in some common antacids to determine their active ingredient, and ask students to show by equations how these particular substances can act as bases. Post answers for the problems and provide students with an opportunity to ask questions pertaining to the problems.

1.4.4 Student Activity: Under teacher guidance, students practise and participate in peer assessment of titration skills including appropriate use and care of burettes. They prepare their own dilutions of an acetic acid solution of known concentration. They then design and conduct a titration to confirm the pH of the solution of acetic acid they have prepared and to calculate Ka.

Teacher Facilitation: The teacher prepares a solution of acetic acid of known concentration for use in the dilutions and a standard base solution for titration.

1.4.5 Student Activity: Students participate in a class discussion about Act 1.4.4. Students work together to solve problems focussing on the use of titration curves for strong and weak acids and bases to determine the pH of the equivalence point. Students complete a written quiz based on Act 1.4 – Acid Base Equilibrium.

Teacher Facilitation: The teacher discusses the results and conclusion from Act 1.4.4. Post answers for the problems and provide students with an opportunity to ask questions pertaining to the problems. Error analysis can also be discussed here. The teacher administers a quiz based on Acid Base Equilibrium.

Assessment & Evaluation of Student Achievement

A laboratory report for the experiment emphasizing the Introduction and Discussion would be appropriate. The teacher could use a rubric as an assessment tool. Students should participate in peer assessment of titration skills. Post or discuss answers to the problems on acid base equilibrium and salt hydrolysis in order to provide feedback to the students. Use a written quiz based on acid base equilibrium to determine the students’ skills.

Report (Inquiry, Communication, Making Connections)
Quiz and/or Problem Set (Knowledge/Understanding, Making Connections, Communication)

Accommodations

·     Use alternative note-taking methods such as a tape recorder.

·     Allow sufficient time for the completion of problems and for students to perform titrations until results are replicated.

·     Set up a buddy system for students during problem-solving sessions.

·     Include illustrations to show proper technique for using the equipment found in this unit.

Resources

Acids and Bases, TVO video series, 1987.

Chem tutor – http://www.chemtutor.com/acid.htm#buffmat
- Acid/base and titration activities

World of Chemistry, TVO Video Series, 1988 – World of Chemistry: Proton of Chemistry

 

Activity 1.5:  Buffer Solutions

Time:  2.5 hours

Description

Students make observations and collect data from a teacher demonstration to help formulate a definition of a buffer system. They enhance their understanding of the characteristics and components of a buffer solution by completing an assigned reading and questions. Students participate in a seminar activity to research and report on how buffering action affects our daily lives.

Strand(s) & Learning Expectations

Strand(s):  Chemical Systems and Equilibrium

Learning Expectations

CSV.01 - demonstrate an understanding of the concept of chemical equilibrium, Le Chatelier’s principle, and solution equilibria;

CSV.03 - explain the importance of chemical equilibrium in various systems, including ecological, biological, and technological systems;

CS1.09 - describe the characteristics and components of a buffer solution;

CS3.03 - explain how buffering action affects our daily lives, using examples;

SIS.06 - compile and interpret data or other information gathered from print, laboratory, and electronic sources, including Internet sites, to research a topic, solve a problem, or support an opinion.

Prior Knowledge & Skills

·     Identify and explain properties of acids, bases, and solutions from SCH3U and SNC2D.

Planning Notes

·     Follow all board regulations for the safe handling and disposal of chemicals.

·     Gather and prepare materials required for Act. 1.5.1: acetic acid, sodium acetate, concentrated acid, concentrated base, pH probe(s) if available.

·     Book time in the resource centre and/or computer room.

·     Gather and prepare questions about buffer systems that incorporate practical applications.

Teaching/Learning Strategies

1.5.1 Student Activity: Students design their own observation chart and collect data from a teacher demonstration illustrating the components and basic characteristics of a buffer system. They generate a definition of a buffer system and hypothesize how it works. Students enhance their understanding by completing an assigned reading and questions.

Teacher Facilitation: The teacher prepares solutions of a sodium acetate/acetic acid buffer system
(6 × 50 mL) and use a pH probe or an indicator to demonstrate the effect of adding small volumes of concentrated acid and base. Remind students to think about the common ion effect and how weak acids function. Direct students to do additional reading and answer assigned questions. Post answers for the problems and provide students with an opportunity to ask questions.

1.5.2 Student Activity: Students research/review material on how buffering action affects our daily lives, e.g., acidosis/alkalosis, buffered medications. Working in small groups they further their understanding by discussing their findings.

Teacher Facilitation: The teacher may book time in the resource centre and/or computer room. Facilitate peer assessment of group work.

Assessment & Evaluation of Student Achievement

A short quiz could be used to ensure that students understand the characteristics and components of a buffer system. It would be appropriate to have students participate in peer assessment of group work skills.

Quiz (Knowledge/Understanding, Making Connections)
Research and/or Report (Inquiry, Communication, Making Connections)

Accommodations

·     Have a range of reading materials for answering assigned questions.

·     Continue the use of a glossary.

Resources

Chem tutor – http://www.chemtutor.com/acid.htm#buffmat - Buffer activities

 

Activity 1.6:  End-of-Unit Task and Written Test

Time:  3.5 hours

Description

This activity is composed of two distinct parts. The first part provides students with an opportunity to combine knowledge and skills acquired throughout the unit to investigate a system at equilibrium. Students design a procedure, make their own solutions, perform a titration, collect and analyse data and communicate their results in a formal laboratory report. The second part is a written test used to assess students’ knowledge and abilities to make connections.

Strand(s) & Learning Expectations

Strand(s):  Chemical Systems and Equilibrium

Learning Expectations

CSV.01 - demonstrate an understanding of the concept of chemical equilibrium, Le Chatelier’s principle, and solution equilibria;

CSV.02 - investigate the behaviour of different equilibrium systems, and solve problems involving the law of chemical equilibrium;

CSV.03 - explain the importance of chemical equilibrium in various systems, including ecological, biological, and technological systems;

SIS.01 - demonstrate an understanding of safe laboratory practices by selecting and applying appropriate techniques for handling, storing, and disposing of laboratory materials, and using appropriate personal protection;

SIS.02 - select appropriate instruments and use them effectively and accurately in collecting observations and data;

SIS.03 - demonstrate the skills required to plan and carry out investigations using laboratory equipment safely, effectively, and accurately.

Prior Knowledge & Skills

·     Students should be familiar with standardizing acids and bases with titration, the common ion effect, Keq, Ksp and Ka and quantitatively determining Keq and Ksp.

Planning Notes

·     Prepare the following solutions at least one week in advance: Ca(OH)2 and Ca(OH)2 with dissolved calcium salt such as Ca(NO3)2.

·     Take proper safety precautions when using concentrated stock solutions.

·     Follow all board regulations for the safe handling and disposal of chemicals.

·     Ensure appropriate materials are available: titration apparatus, filter paper, indicators, thermometers, concentrated hydrochloric acid.

·     Prepare a written test that assesses students’ knowledge and ability to make connections.

Teaching/Learning Strategies

1.6.1 Student Activity: Students use their knowledge of Ksp to design and conduct an experiment to determine the solubility product constant for a semi-soluble salt, such as Ca(OH)2. Students should then use their knowledge of the common ion effect to determine the additional calcium ion concentration in an equilibrium system, e.g., Ca(OH)2 containing dissolved calcium salt. This activity provides students with an opportunity to link skills and knowledge used throughout the unit, such as, using appropriate safety procedures, applying Le Chatelier’s principle, and performing a titration.

Teacher Facilitation: Prepare two solutions, Ca(OH)2 and Ca(OH)2 with dissolved calcium salt, at least one week prior to use. Review the evaluation scheme with the class. Encourage students to consider using methods or techniques to maximize accuracy, e.g., filtering the Ca(OH)2 solutions, using three trials etc. Ca(OH)2 is corrosive. Remind students to handle and dispose of chemicals safely. The teacher may also allot time during the activity to assess the students’ practical skills.

1.6.2 Student Activity: Students complete a written test.

Teacher Facilitation: The teacher generates a test focussing on Knowledge and Making Connections.

Assessment & Evaluation of Student Achievement

A formal laboratory report for the experiment would be appropriate, since it helps prepare the student for the Final Assessment Task. A written test including a variety of types of questions could be used to assess the student’s knowledge and ability to make connections.

Report (Inquiry, Communication, Making Connections)
Unit Test (Knowledge/Understanding, Making Connections)

Accommodations

·     Provide identified students with extra time for the written test.

·     See Accommodations in the Course Overview.

 

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